Deposition of TiO2/PT Composite Particles Using Pulsed Laser Deposition Technique

https://doi.org/10.24237/djes.2016.09307

Authors

  • Amin Daway Thamir Production and Metallurgy Engineering Department, University of Technology
  • Adawiya J. Haider Center of Nanotechnology, University of Technology
  • Ghalib A. Ali Production and Metallurgy Engineering Department, University of Technology

Keywords:

Pulsed Laser Deposition Technique, Pt doped TiO2

Abstract

In the present work, the titanium oxide platinum (TiO2/Pt) composite particles were deposited on the Si and glass substrates at (400)°C using pulsed laser deposition technique to ablation of TiO2 target at constant laser energy 800 mJ, a double frequency Q-switching Nd: YAG laser beam ( λ= 532 nm, repetition rate 6Hz and the pulsed duration 10ns). Ultraviolet visible (UV-Vis) spectroscopy, X-ray diffraction (XRD),X-ray fluorescence (XRF), Atomic force microscopy (AFM),Scanning Electron Microscopy (SEM), electrical conductivity (σdc), Hall coefficient (RH) ,(I-V) and (C-V) were used to characterize the morphology and electrical of the films. The results showed that the transparency of film reached to about (80%) with optical band gap (3.64) and (3.76) eV for Pure TiO2 and 5% Pt:TiO2 respectively. The structural and composition of the obtained films at level 5% of platinum doping into TiO2 have been determined. The results indicated that the prepared films (Pt doped TiO2) were nanostructure and uniform with diameters less than 20 nm.

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References

R.B. Zhang, L. Gao, (2002), Key Eng. Mater. 573, 224–226.

B. Klingenberg, M.A. Vannice, (1996), Chem. Mater. 8, 2755.

Y.Gao,Y.Masuda,Z.Peng,T.Yonezawa,K.Koumoto,J.(2003), Mater.Chem.13608.

S.A. Sher Shah, A.R. Park, K. Zhang, J.H. Park, P.J. Yoo, (2012),ACS Appl. Mater.Interfaces 4 3893 .

K. Chhor, J.F. Bocquet, C. Pommier, (1992), Mater. Chem. Phys. 32 249.

A.Larbot,I.Laaziz,J.Marignan,J.F.Quinson,J.(1992), Non-Cryst.Solids147157

A. J. Haider et al., 01 June (2011)," Nanostructure dopants TiO2 films for gas sensing", Iraqi Journal Applied Physics,.

A. J. Haider et al (2012)," Effect of Oxygen Pressure on the Optical, Morphology and Structural Properties of TiO2: Cr Thin Films Prepared by Pulsed Laser Deposition ", Journal of Materials Science and Engineering A 2 (3) 346-351.

S.S.Kaduory et al., (2013),"Annealing Effect on the Growth of Nanostructured TiO2 Thin Films byPulsed Laser Deposition (PLD) " ,Eng. & tech. Jour nal .Vol31, Par t (B), No.4, .

T. Ivanova, et al., (2013), Optical Materials 36 207–213 .

D. K. Pallottiet et al. , (2013).Journal of Applied Physics 114, 043503

K. Z.Yahya et al, (2014),"Effect of Substrate Temperature on Nanostructure Titanium Dioxide Thin Films Prepared by PLD ", Eng. &Tech.Journal, Vol.32, Part (B),No.3,.

L. sun et al.,(2009),Separation and Purification Technology 68 83-89 .

S.Aksoy and Y. Caglar,(2014),Journal of Alloys and Compounds 613 330–337.

Published

2016-09-01

How to Cite

[1]
A. D. Thamir, Adawiya J. Haider, and G. A. Ali, “Deposition of TiO2/PT Composite Particles Using Pulsed Laser Deposition Technique ”, DJES, vol. 9, no. 3, pp. 81–89, Sep. 2016.